ThreePointCircle
Bluelighter
- Joined
- Apr 21, 2016
- Messages
- 331
312.png sample . Self synth safrole via benz wacker batch... pretty sure dis one as we ran the Hell out of that NMR. the one Vecktor did nov. 18th ish@vash445 Wow! So was that originally the ...579.pdf sample or the ...312.png sample? And yeah, that's looking a lot more like the magic sample, and the MDMA NMR references online (e.g. the UN doc)
@vash445 right, got you. Very exciting.
My knowledge of such things is limited but after going through the column you have several fractions right? Any possibility of doing the NMR on the other fractions to get a 'clean' view of the contaminant that was originally present?
So, theoretically, something was there in addition to the MDMA that was largely flying under the radar, and the silica column cleared it? What is a silica column and is that something people could try on their own product?
No idea, sorry mate I asked if he still has the layers to investigate, the amount of product was only 1-2 grams so I don't expect much solvent anyways
*edit he said he has the solvent still but the product was already pretty clean to begin with...
I was looking at a couple of videos, and the first one they didn't use any kind of pump - just let gravity do its thing. Is this feasible? And what solvent did you use?Vacuum Pump - 12V: Industrial Products: Amazon.com: Industrial & Scientific
Vacuum Pump - 12V: Industrial Products: Amazon.com: Industrial & Scientificwww.amazon.com
I was looking at a couple of videos, and the first one they didn't use any kind of pump - just let gravity do its thing. Is this feasible? And what solvent did you use?
Once you've got your fractions, could we just use reagents to locate the mdma? Or is that too rough a procedure.
Thanks. I'm guessing that's Methanol : DCM. Any info on the ratio?Standard size for flash column (230-400 mesh) 40-63 um with a 60 angstrom . Solvent denatured Methanol:DCM
Thanks. I'm guessing that's Methanol : DCM. Any info on the ratio?
No worries. Thanks for all your help - it's been a great step forward.no idea on ratio sorry`, I imagine it is highly column dependent. Is the elute staying up top you probably need more MEOH etc. etc. This isn't my speciality sorry
Great. I'd love to help but not sure what I can do. I was thinking about the recrystallisation but since you've had success converting a sample, I'm thinking I should give the chromatography a go. All a bit of a learning curve but oh well, hopefully it'll be well worth it.
I'd be up for giving a donationWe also plan on setting up a bitcoin and monero address for donations to run the NMR.
From a cursory glance at r/mdma it seems like everyone there is getting magic stuff..
MagicMDMA, you just accept that MehMDMA is what MDMA experience should be.