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The Big & Dandy N,N-DMT Extraction Thread - Elves are watching

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tan-ish brown gooey stuff?? HMMM...could be basic mimosa goop, or it could be tannins from the mimosa...ph paper it??? But I'd smoke it...lol...ph test it first though really, worst it can be is a bit harsh, I'm sure it's not much more harmful than inhaling DMT fvapour.
 
Hey Jblazing; This might be lazy of me, but after sifting through 7 pages of your posts I decided it would be more expeditious to just ask, what kind of tek are you using? This'll be my 3rd extract and I'm just trying to explore what works well for others. Your product looks phenomenal, I must say
 
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Hahahahah

STB. It took me quite a few goes - like 5 to get it that nice and clean.

That was with my last 120g of MHRB.

Basically if you don't fuck about, you use this ratio of ingredients MHRB:NaOH:H2O 1g:1~:15ml with each solvent pull heated for a few minutes, and all done in one session - the solvent I usually used between 70 & 100ml each pull.

THEN you will be able to get clean product.

For the last of my kilo, I personally did 3 pulls with clean solvent and the last pull with solvent which still had some DMT which wasn't precip'd out in it to make the saturation better for freezing.

I also left the jars in the freezer for 24 hours after 2-0.5-2-0.5 hours fridge - freezer.

I poured the solvent through a coffee filter into a glass where the floating DMT got caught, after I shook the jar vigorously.

THen all the DMT stuck to the bottom and sides - I squirted hot solvent onto(light petroleum distillate in the form of Zippo lighter fluid), then poured it out and evaporated that in a glass dish, covered with a few coffee filters so as to allow air but no dust to permeate - yielding those beautiful shards and crystal formations.

Can't wait til my next extraction - going to be this week hopefully if I can get a vendor to sort me out with some bark within 2-3 days.

I haven't smoked any DMT in like 4 weeks - I really wanna do some art based on my visuals etc, and writings, so I wanna get started again, especially considering I got the technique down through keeping my attention focussed for a few hours haha.

PEACE
 
Thanks for the reply. I'm assuming your 70-100 ml of solvent per pull was for 120g of bark? I used the same MHRB:NaOH:H2O ratio, more naptha (1mL/g), but I've had some disappointing yields. Guess my technique needs refinement. Or my source material isn't up to par. (I'm leaning more towards part of my technique being the problem) I'm hoping my next extraction goes better. I'll probably allow my solvent more time to pull before siphoning it off as my most successful pull was the one allowed the most time.
 
FOr the first 2 pulls don't leave it too long - not much longer than half an hour.
FOr the 3rd (and 4th if you think it's necessary) leave it in there for a few hours, shaking every half hour or so.

Oh and remember to keep it warm!!

Peace
 
psilocybonaut said:
If a kilo is DONE CORRECTLY, it could yield 10 grams of clean DMT. Refer to my reply here on proper extraction techniques (only doing 28g powdered MHRB/jar, doing at least 4 pulls per jar, etc. just read it, for a kilo you will need to do 36 separate mason jars with 28g in each)
Click to expand...

I would be unhappy with a 1% yield (although I'd got once 0.7% ) I usually get 1.2-1.6%, so between 12 and 16 grams with 1kg of MHRB
 
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Elf Spice Extraction TEK
by HeartCore
Wednesday, 11 October 2006

....seems nice and easy what with the pics

Only thing is its for 250 grams mhrb

how would one change the quantities for 50g - surely not as simple as divide everything by 5, even the water?
 
if you do not have a crockpot, how high should flames by on a gas HOB?

should stuff be simmering not bubbling?

Or even lower than a simmer?

How hot should the water be?
 
Are you talking an ayahuasca brew or a freebase extraction?

If it's ayahuasca you want to just simmer it, don't let it get boiling that's a bit too hot.



If you are talking a freebase extraction you should not be working near an open flame while using highly flammable solvent.
 
mi5 said:
Elf Spice Extraction TEK
by HeartCore
Wednesday, 11 October 2006

....seems nice and easy what with the pics

Only thing is its for 250 grams mhrb

how would one change the quantities for 50g - surely not as simple as divide everything by 5, even the water?
Click to expand...


It really is that simple, think about it like cooking. If you want 1/4 of the amount of cookies called for in a recipe you just use 1/4 the amount of ingredients in the same ratios.... come on man.
 
adrian89987 said:
If you are talking a freebase extraction you should not be working near an open flame while using highly flammable solvent.
Click to expand...


but the early step where you just have water vinegar mhrb mixed together...surely is meant to be hot?
 
Ah sorry, didn't realize it was an A/B tek. Well a similar heat as for ayahuasca really. Simmer it for a bit.
 
is 25g too low to bother with?

a first timer should use 25 one time then 25 another time - tp get the hang of it...


or just go all in with their 50?
 
I wouldn't even do 50 to be honest - it's not hard to do honestly if you just follow a good tek - gir's one with a pictoral on dmt-nexus is pretty good (STB) and I'm sure you can find a good one for A/B there to follow - and if you just follow it to the letter, you'll have some great DMT.

I'd use 125 personally.
 
weird extraction pull times

I've been having the WEIRDEST extraction yet since I got my technique really crisp and easy to perform in a few hours, this new batch of mimosa yielded the most insane 1st pull - started crystallizing fat spikey rocks at room temperature after a few hours!! Problem is the pulls are taking fucking AGES to seperate...I don't understand why, I been using heated naptha for all pulls after the first (forgot here), and have kept it warm using lye.

:\
 
I have a weird one going too, well, unexpected anyway. The 4th and final pull seems to be the most concentrated. The first three are obviously in need of a partial evap before a freeze precip as not many crystals crashed out. Sigh. I'm gonna get this down one way or another. lol
 
Is there any sort of correlation between the color of your solvent (naptha) and the yields? I just put my naptha in the freezer, and it definitely had a yellow tint to it.

I ask because this is my first time giving it a real go. I've made half-assed attempts in the past, but this is the first time I'm really trying to get some good yields.
 
Yellow tends to correspond to plant oils being extracted. These oils are usually less soluble in the solvent than the DMT though so that could be a sign that yes you have extracted a bit of stuff out of your plant.
 
4 pulls freezing right now.... starting to look good, though not as nice of a yield as I would like.....

Then again, I have done quite a few things differently this time in order to attempt to get larger, cleaner crystals, so that may be why the yield is so low right now.... (looking, havent measured yet)


This time, I used room temp solvent and did really quick pulls (less than 30 minutes, only one or two mixes durring this time)

I also wrapped the containers that are holding my NPS and my crystals really thickly with cling wrap, to try to insulate the container and slow the freezing process down.

My solvent for each pull came out perfectly clear, rather than the typical yellow it comes back as.....


Anyways, my goal is to end up with fairly pure DMT, while not totally spending the bark so that I can later come back to it and try a full range extraction....

Is it correct to think that room temp solvent will absorb less impurities than warm solvent? I know that room temp solvent will dissolve less than warm solvent, but dont really know enough about the solubility of everything contained in mimosa hostillis rootbark to know for sure....
 
Does anyone happen to know the solubility of DMT in naptha at low temps? After my freeze precipitations I've evapped my solvent and been left with such little crystal that it isn't worth my time to scrape it up, so it SEEMS that solubility approaches zero at extremely low temps. Could anyone corroborate this? With such little DMT left in the solvent after a freeze precip I'm not sure I can justify reusing it for additional pulls since it is also holding impurities, aside from getting as much use out of a hazardous product as I can and not being wasteful with it. Anyone have any thoughts on this?
 
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