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The Big & Dandy N,N-DMT Extraction Thread - Elves are watching

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can the bark be thrown straight in the bin afterwards, covered in lye and all that shit?
 
I would not throw that into the trash.


What you need to do is dilute it a shit load, and then flush it.
 
Finished my first attempt on an extraction yesterday and got a nice pile of yellowish crystals.
Did a 20 mg test in a small pipe. Wasn't really expecting much, but damn I got a surprice!
The speed of the onset totally blew me away. I was instantly but in a very different place :) Not a full breakthrough, but close.

Can't wait to do some experimenting on the extraction method and further testing off course.
 
Ellis Dee said:
I used the TEK you posted with the HDPE 2 milk jug. I have done 2 fresh extractions since the botched attempt both on 100g of fresh new bark. Each of these last attempts yeilded 300-500 mgs pure white crystal. I followed the TEK you posted exactly. I still have the milk jug containing the basified MHRB after having done 4 pulls all 75 ml, then combined in a pyrex tray and evaporated down to 50 ml total. when put in the freezer this yeilded 300ish mgs.
Click to expand...

I normally freeze precipitate all my pulls separately so I can tell that by the fourth one that it's not worth the hassle of doing another. You could try one more pull of 75ml and see if anything drops out in the freezer that you might have missed.

I'm just looking through the tek to see what i've changed since I first started out.

step 2 - Lye, I don't weigh it but I know im getting around 100g due to the container I buy it in.
step 5 - I always let the lye, bark, water mix sit for 2 hours
step 6.5 - I don't heat the naptha unless it's just come out the freezer from a previous pull, if i want to do another pull right away I will put it in a warm water bath to bring it up to room temperature only, no warmer.
step 7 - I use 120ml naptha per pull. I don't roll the mix end over end, i give it a good slow shake and let it seperate a few times for about 15 mins before pulling.
step 10 - I don't leave a pull in the freezer overnight, I may have a very cold freezer but within 3 hours all the crystals have dropped out, so I am ready to use the naptha for another pull.
step 11 - I don't recrystallise. never felt the need as I get very nice white crystals.

I'm not sure that these changes will make much difference to you as I got nearly a gram the first time I tried and I followed that tek pretty closely, they just seem more convenient for me.
Maybe you were right about the bark not being the best, try a different source.

Peace
 
ColtDan said:
can the bark be thrown straight in the bin afterwards, covered in lye and all that shit?
Click to expand...

Lye is actually used as a drain cleaner, I just flush it down the loo, wear your safety gear and pour it in there carefully though to avoid splashback on walls etc.
Take it from me this stuff will strip paint.
 
It comes in a plastic container so why not.
As I have said in an earlier post i use a well rinsed hdpe2 plastic milk container and throw it away and use a new one for each batch, it would probably be fine to use again but they cost me nothing so why not.
I have left the lye solution in one for over a week without problem the only thing i don't trust is the lid as it is made from a different plastic and I guess it could degrade over time.
That container you linked to looks large and unwieldy how much bark are you extracting?
 
just added lye to water, then the root bark, only got around to adding a small amount of naptha before i go interrupted and cant continue doing the experiment tonight. will it be ok to carry on adding the rest of the lighter fluid tomorrow?
 
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how much did you add?? Why not just wait, and do it later?? Unless you're having sex - your parents will go to bed...or what, why not just finish it??!!? the solution should still be nice and warm you can do 2 pulls before you go to bed. Best time to do it, otherwise tomorrow you'll have to reheat/add more lye, a lot more.:\
 
yeah that is my ratio. so i have to re-add another 100g... fuck sake. will nothing happen if i add more lighter fluid tomorrow without adding more lye?
 
it will - it's just now that you have heat you have a reaction which doesn't take days to seperate the naptha...just like half an hour.

you WON'T have to add another 100g. I'd say half though, I tried adding like 25-30g and it didn't heat it up much...fuck it, you MAY have to add another 100g for all I know, I don't do it that way anymore I just let it sit for longer, and give it more shakes, let it settle then seperate.

Missions - need to try and do it all in one sitting, works a LOT quicker that way trussssss
 
so wait you added 100g to 100g of mhrb, added naptha then got interrupted? is this right?

you don't have to add any more lye if so, just pull the naptha
 
ok just added 30g more lye to heat it up, then added the rest of the naptha. only got around to adding about 30ml yesterday, dumped the entire 120ml in there just now. just swilled it around gently, turned it end over end. gonna leave it for a bit and try and syphon the top later off later. not in a huge rush, got all day to get this done. hope i havent fucked anything up
 
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