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questions about DMT extraction from accacia obtusiflora

shiam

Bluelighter
Joined
Dec 21, 2005
Messages
38
my freind was wondering if any experts can help him out with his extractions
my freind used citric acid on approx 150g of bark for the first part of the extraction
he then cleaned the solution with naptha
he then tried to basify the solution using caustic soda
this is where he is a bit confused... all the techs he has read say that the solution should turn greyish and then pinkish , this did not happen, he noticed where drops of base were added the solution would become a dark red but would then dissappear with stirring, the solution would become darker but that is all. after adding more naptha and stirring, the solution separated into two layers one the dark red solution, the other a perfectly clear layer of naptha.
apon evaporation all that was left was what appeared to be some yellowish oily substance and when this dried out there was nothing left in the evaporating dish.

he has since tried this again but with similar results though the last time it appeared like there might actually be an extremely small amount of something that had a distinct synthetic smell though he suspects there is not enough for an active dose (if what he has is DMT)

he also noticed apon his second attempt than when the naptha was evaporating there was a whiteish/greyish cloudiness to the solution that seemed to occur when the naptha evaporated (more of this white cloudy stuff would appear when the naptha was fanned then it would sink and dissapear)

is he doing something wrong? any advice would be helpfull
 
oh yeah after the first extraction didnt work he just left some jars containing the basified solution sitting around lids on etc.
he noticed that dark red clouds of somthing had settled to the bottom of the jar. he wanted to know if one was to evaporate off the base solution whether you would have some crude from of DMT, so that he could skip the final naptha step alltogether
 
he said he'd give it a try but he thinks he raised the ph to well above 14 and it didnt change, he was also worried that if he over basifies he might destroy the DMT
 
ok well maybe not well over 14 but definatly in that region because his universal indicator paper only goes to about 14 and he kept adding base after that because it didnt seem to change any more
 
he says its a bloody pain in the ass cos he knows he's close theres just something he not doing right
any word on what would happen if he just evaporated the basified aqueos solution ?
 
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