futura2012
Bluelighter
I see we now have two pills of the 90s threads... LOL
Re the GC/MS tests of pills. I dug into this a little further: Sorry for the long link
http://www.documentingreality.com/f...7YCwDA&usg=AFQjCNGhiNhfLDzXSj9f3Tb86sw8B1i0nQ
Forensic Investigation of Clandestine Laboratories Donnell R. Christian (an interesting read)
Would seem the Gas Chromatography could if needed seperate the isomers for analysis.
Ref PG133
"The GC can be used to differentiate geometric isomers. An example of the use of GC retention times to differentiate between isomers is the identification of the cis- and trans-phenylaziradines that are by-products of the HI reduction of ephedrine to methamphetamine. Even though these compounds have essentially the same mass spectrum, the GC retention times are significantly different."
However I am not so sure the Mass Spectroscopy is going to figure out the Salt Type of MDMA by seperating the ionic bond and then analysing it.
Ref PG134
"The mass spectrometer generally cannot distinguish between the salt and freebase form of a drug. The salt portion of the compound is generally outside the detection range of the MS. The detector only “sees” the freebase portion of the compound."
even if the GCMS could see an identified acid couldnt it be mistakened with another spike? Perhaps an impurity in the synth?
I cant see how a pill analysis site such as ecstasydata.org is going to look too heavily into the actual salt type or the isomers of MDMA.
One simple reason would be time it would take.
I was reading in there 'About Tests and Data Section'
"Why don't you display actual milligram quantitative amounts?"
"In short, the DEA does not allow us to do so. In the United States, the handling of Schedule I substances (MDMA, LSD, Cannabis, etc) is restricted to those with a valid DEA license. Forensic labs such as DDL and others require DEA licensure in order to operate. The DEA has made an unpublished administrative rule that licensed labs are not allowed to provide quantitative data to the public, reportedly for fear of providing 'quality control' to dealers and suppliers of black market products."
If the DEA forbids mG quantities being represented I can only assume that reports suggesting Isomers, salt type etc might fall within this ban.
Clearly this is only valid for the USA but I am still not convinced these lab reports are going to shed a true light on the isomer ratio or salt type a pill might contain.
Have methods for manufacturing MDMA and pills in the 90s changed from methods now? Highly likely
Were pills in the 90s better than pills today?
In America and Australia you could argue - Yes
In Europe you could argue - No
but.. they were different - For Sure
Does a coctail of MDA, MDEA, MDMA make a good pill? - Stronger Yes Good? Very Much Personal Opinion
Is the compared high of a 90s pill to a pill now just down to fried brain / down regulation / memory and nostalgia - UNLIKELY
Which general pill type is better 90s or Now - To be continued...
Just out of interest has anyone had first hand experience of Defqon/Speaker/Triforce/Squirrel/QDance would be really interested to know how the actual buzz compared.
Re the GC/MS tests of pills. I dug into this a little further: Sorry for the long link
http://www.documentingreality.com/f...7YCwDA&usg=AFQjCNGhiNhfLDzXSj9f3Tb86sw8B1i0nQ
Forensic Investigation of Clandestine Laboratories Donnell R. Christian (an interesting read)
Would seem the Gas Chromatography could if needed seperate the isomers for analysis.
Ref PG133
"The GC can be used to differentiate geometric isomers. An example of the use of GC retention times to differentiate between isomers is the identification of the cis- and trans-phenylaziradines that are by-products of the HI reduction of ephedrine to methamphetamine. Even though these compounds have essentially the same mass spectrum, the GC retention times are significantly different."
However I am not so sure the Mass Spectroscopy is going to figure out the Salt Type of MDMA by seperating the ionic bond and then analysing it.
Ref PG134
"The mass spectrometer generally cannot distinguish between the salt and freebase form of a drug. The salt portion of the compound is generally outside the detection range of the MS. The detector only “sees” the freebase portion of the compound."
even if the GCMS could see an identified acid couldnt it be mistakened with another spike? Perhaps an impurity in the synth?
I cant see how a pill analysis site such as ecstasydata.org is going to look too heavily into the actual salt type or the isomers of MDMA.
One simple reason would be time it would take.
I was reading in there 'About Tests and Data Section'
"Why don't you display actual milligram quantitative amounts?"
"In short, the DEA does not allow us to do so. In the United States, the handling of Schedule I substances (MDMA, LSD, Cannabis, etc) is restricted to those with a valid DEA license. Forensic labs such as DDL and others require DEA licensure in order to operate. The DEA has made an unpublished administrative rule that licensed labs are not allowed to provide quantitative data to the public, reportedly for fear of providing 'quality control' to dealers and suppliers of black market products."
If the DEA forbids mG quantities being represented I can only assume that reports suggesting Isomers, salt type etc might fall within this ban.
Clearly this is only valid for the USA but I am still not convinced these lab reports are going to shed a true light on the isomer ratio or salt type a pill might contain.
Have methods for manufacturing MDMA and pills in the 90s changed from methods now? Highly likely
Were pills in the 90s better than pills today?
In America and Australia you could argue - Yes
In Europe you could argue - No
but.. they were different - For Sure
Does a coctail of MDA, MDEA, MDMA make a good pill? - Stronger Yes Good? Very Much Personal Opinion
Is the compared high of a 90s pill to a pill now just down to fried brain / down regulation / memory and nostalgia - UNLIKELY
Which general pill type is better 90s or Now - To be continued...
Just out of interest has anyone had first hand experience of Defqon/Speaker/Triforce/Squirrel/QDance would be really interested to know how the actual buzz compared.

