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Which PiHKAL and TiHKAL substances can be smoked as freebase

5-MeO-DALT can be smoked (and taken intra-nasally as well). While it is not exactly a PiHKAL or TiHKAL substance, it is one of Shulgin's creations and is said to appear in "The Shulgin Index".

I have only limited experience smoking the substance, but it works well and lasts for a few minutes. Intra-nasally lasts longer but is far less intense. I prefer oral or intra-nasal administration though.
 
There are a couple smoked 5-meo-mipt reports in TIHKAL, also a couple for DET if I recall.
 
i think alot of the non substituted tryptamines can be smoked.

also ive heard of 2c's being smoked but it wasnt a very popular method.

Even their salts can be smoked if you're really careful while heating them.
 
5-MeO-AMT can be smoked as well... As can 5-MeO-MET and I believe that 5-MeO-AET was smokable as well but don't quote me on that.

Now out of the list, which ones are PLEASURABLE?

AMT
MiPT
5-MeO-AMT (less bodyload, way faster visuals than you get orally, no diarrhea, very light nausea)

Those are the ones I've personally smoked and enjoyed. I've tried smoking just about all of them back in my stupider days.

5-MeO-MiPT
5-MeO-DMT
5-MeO-DiPT
DiPT

Those were not pleasant experiences and I would not repeat them. 5-MeO-DiPT was an accident, it was supposed to be 5-MeO-DMT but my buddy got out the wrong vial - after obtaining no effects from it, we realized what was wrong. 5-MeO-MiPT was actually visual smoked but we smoked too much (6mg) and had a rather unpleasant stimulation and we both puked our guts out. DiPT as I remember didn't do much though we didn't smoke a lot of it, it was just an experiment. As DiPT tends to be a higher dose chem, it probably would have worked at higher levels.

Let me just say though... Smoking hydrochloride salts is NOT pleasant and it is extremely harsh on the lungs...
 
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