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  • BDD Moderators: Keif’ Richards

trouble with wacker oxidation

Rocksteady3232

Greenlighter
Joined
Apr 11, 2012
Messages
39
Location
PacNorthWest
A foaf is having trouble in the wacker oxidation process. He added 700ml dimethylformamide, 100ml dH2O, 17.5g Palladium Chloride, and 170g cupric chloride to his three neck flask....now the issue is that he didnt have the stirring on durring the addition, and the cupric and palladium have now formed a solid cake on the bottom of his flask!

Does anyone know what is happening and what to do about it???!!?!?!??! Please any thoughts may help and time is of the essence.
 
i dont know what a foaf is.

but this semes better suited to advanced drug discussion as i have absolutely no idea what you're talking about.
 
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