Hello,
I have few questions about the recrystallization. I've tried with all solvents that i had access , ethanol and methanol looks to be the best .
With water , there's something that i miss for sure , i don't know what to do with it , ?
I just got ether , should i do it with this instead of ethanol and methanol ?
And toluene? if i mix water and toluene , where's my compound? how can i extract it ?
Should i wash it with acetone before starting the recrystallization?
Should i cover my flask wright after boiling and start to cool down?
Freezer , counter or ice bath is the best to cool down?
Is there'S tricks to make big and solids shards?
Do the erlemyer is a good choice the cook a small batch ?
hope someone will give me good tricks so i can finally make something good for me !
Thanks
I have few questions about the recrystallization. I've tried with all solvents that i had access , ethanol and methanol looks to be the best .
With water , there's something that i miss for sure , i don't know what to do with it , ?
I just got ether , should i do it with this instead of ethanol and methanol ?
And toluene? if i mix water and toluene , where's my compound? how can i extract it ?
Should i wash it with acetone before starting the recrystallization?
Should i cover my flask wright after boiling and start to cool down?
Freezer , counter or ice bath is the best to cool down?
Is there'S tricks to make big and solids shards?
Do the erlemyer is a good choice the cook a small batch ?
hope someone will give me good tricks so i can finally make something good for me !
Thanks