fifo_thekid
Greenlighter
- Joined
- Oct 9, 2015
- Messages
- 18
So, I could get the Ammonia. I did exactly the following:
1- Dissolved 4g in about 50ml of water and filtered it with a cafe filter. After filtering I poured some more water and pressed the paper well to make sure that nococaine was left behind. I was left with so much insoluble crap that has no taste, smells like kerosene, and has orange color.
2- With a total of about 80ml of water with cocaine that looks semi clear, I diluted 28% ammonia to 10% and started dripping slowly, clouds started forming in the liquid. I continued mixing a little and dripping a little until the precipitation stopped and the liquid started smelling like ammonia. the pH at that time was around 8-9. I should have boiled the water before adding the ammonia but I forgot to do that.
3- Filtered the solution through coffee filter, and most of the whitish base got stuck in filter. This result was a million times better than with the sodium bicarbonate. Then I poured about 50ml of hexane into the beaker that I used for preparing the base to make sure that whatever was left behind is dissolved, and then washed the filter with hexane and squeezed it well into the beaker.
4- Added 20ml of water to the available 80ml of hexane, shacked well, then started moving the beaker in circular motion. Two layers were formed: the lower one had cloudy water (Levamisole?), and the upper one had clear hexane with cocaine base dissolved in it. Pulled the lower water layer with a syringe and threw it away. Then, I poured the hexane in a large transparent plate and put it on a boiled water path to accelerate the evaporation of hexane (evaporates at 68 degrees). Within minutes I was left with a plate full of white residue, and to my surprise, this super clean cocaine base had a high yield! At that moment I was so happy, especially when I smoked some and found that it was THE BEST CRACK/BASE I'VE EVER TASTED!
Then from here, everything went downhill....
5-Dissolved the base into 80ml of anhydrous acetone (although I had magnesium sulfate, but I was in a rush and I didn't want to wait for 4 hours for it to be dehumidified in order to remove all the water from acetone), when all the cocaine base was dissolved, I added some drops of 32% hydrochloric acid, mixed a little, waited, nothing happened! Added some more drops, mixed a little, waited for half an hour, and nothing happened!
Checked the pH, and it was below 1! So I added a little Everclear, mixed, waited for an hour, and still nothing! Only clear liquid.
I put the mix into a big plate and under the sun, until all the acetone was gone. I was left with a little water, HCL, and MOLTEN LITMUS PAPER!
Heated it in the oven, the the HCL was transformed into suffocating gas. Put it again in the microwave, and I was left with reddish sludge (red from the litmus paper!!). I tried scraping it, and to my surprise I found that the quantity now was much lower, although I didn't pass the liquid through any filter, and the final product was a mix of cocaine base AND cocaine HCL, wit about 50:50 ratio. However, the quality was so bad as it still had molten paper and HCL...aaaaaaaaaaaaand it went to the trash :'(
Next I'm trying to follow everything up to step 4, taking care of my previous mistakes, but in step 5 I'd make a 1:2 mix of HCL and hexane and add it to anhydrous acetone completely dried.....
Any Advice would be appreciated
1- Dissolved 4g in about 50ml of water and filtered it with a cafe filter. After filtering I poured some more water and pressed the paper well to make sure that nococaine was left behind. I was left with so much insoluble crap that has no taste, smells like kerosene, and has orange color.
2- With a total of about 80ml of water with cocaine that looks semi clear, I diluted 28% ammonia to 10% and started dripping slowly, clouds started forming in the liquid. I continued mixing a little and dripping a little until the precipitation stopped and the liquid started smelling like ammonia. the pH at that time was around 8-9. I should have boiled the water before adding the ammonia but I forgot to do that.
3- Filtered the solution through coffee filter, and most of the whitish base got stuck in filter. This result was a million times better than with the sodium bicarbonate. Then I poured about 50ml of hexane into the beaker that I used for preparing the base to make sure that whatever was left behind is dissolved, and then washed the filter with hexane and squeezed it well into the beaker.
4- Added 20ml of water to the available 80ml of hexane, shacked well, then started moving the beaker in circular motion. Two layers were formed: the lower one had cloudy water (Levamisole?), and the upper one had clear hexane with cocaine base dissolved in it. Pulled the lower water layer with a syringe and threw it away. Then, I poured the hexane in a large transparent plate and put it on a boiled water path to accelerate the evaporation of hexane (evaporates at 68 degrees). Within minutes I was left with a plate full of white residue, and to my surprise, this super clean cocaine base had a high yield! At that moment I was so happy, especially when I smoked some and found that it was THE BEST CRACK/BASE I'VE EVER TASTED!
Then from here, everything went downhill....
5-Dissolved the base into 80ml of anhydrous acetone (although I had magnesium sulfate, but I was in a rush and I didn't want to wait for 4 hours for it to be dehumidified in order to remove all the water from acetone), when all the cocaine base was dissolved, I added some drops of 32% hydrochloric acid, mixed a little, waited, nothing happened! Added some more drops, mixed a little, waited for half an hour, and nothing happened!
Checked the pH, and it was below 1! So I added a little Everclear, mixed, waited for an hour, and still nothing! Only clear liquid.
I put the mix into a big plate and under the sun, until all the acetone was gone. I was left with a little water, HCL, and MOLTEN LITMUS PAPER!
Heated it in the oven, the the HCL was transformed into suffocating gas. Put it again in the microwave, and I was left with reddish sludge (red from the litmus paper!!). I tried scraping it, and to my surprise I found that the quantity now was much lower, although I didn't pass the liquid through any filter, and the final product was a mix of cocaine base AND cocaine HCL, wit about 50:50 ratio. However, the quality was so bad as it still had molten paper and HCL...aaaaaaaaaaaaand it went to the trash :'(
Next I'm trying to follow everything up to step 4, taking care of my previous mistakes, but in step 5 I'd make a 1:2 mix of HCL and hexane and add it to anhydrous acetone completely dried.....
Any Advice would be appreciated