He was referring to taking the LSD as the MDMA was wearing off.
From PIHKAL....
>The putting of a drug on top of an active drug, usually
>during the latter part of its effectiveness is, as previously
stated, called "piggy-backing."
>EXTENSIONS AND COMMENTARY: There is need for more commentary.
>It must be noted that all of the above comments used rather modest
>dosages of LSD. The notes of this period, some two years of exploring
>interactions of the MD series of compounds as preludes to true psychedelics,
>are difficult to distill into a simple pattern. Most of these studies used LSD in
>the 60-100 microgram range which is fundamentally a modest level. Many
>trials were made where the challenge of acid plopped right on top of an
>active residue of another drug was more in keeping with the "piggyback"
>argument. An illustration of this is a trial in which the primer was MDMA
>followed at 5 hours (this is at a time of almost no effect) with a larger dose of LSD
What did he mean by "post-MDMA"? The day after? Or when the MDMA was wearing off?
I wouldn't be so keen take Shulgins work as law - taking LSD at the end of a heavy MDMA session when you're already exhausted - meaning you're going to be awake for another 12-24 hours sounds like a waste of LSD to me. Not great for your health either.
Any idea why he was only taking 65ug? That's not really a psychedelic dose anyway - was he taking that because he knew LSD didn't become psychedelic after MDMA no matter what dose he took?
.
I personally prefer to take LSD first, MDMA one hour later...but I have done it the other way around and what you say just was not my experience. MDMA never particularly makes me exhausted anyway (beyond having stayed up all night), but taking a psychedelic on the tail end (LSD numerous times, 2C-I on one occasion, and 2C-T-7 a couple or three times in my case) is very enjoyable and not at all 'rough' or a producer of a more severe hangover.