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Cocaine Purification help!

eddiecoleman

Greenlighter
Joined
Apr 27, 2026
Messages
2
After some bad experiences with side effects like an extremely sore nose and bad comedowns I ended up on a le junk and David le rabbit hole to try and get rid of some the sh*t in my gear.

I've done an acetone wash and a/b procedure (somewhat successfully I believe) which leaves me with freebase. Turning it back into a snortable sort is where I'm getting grief.

I'm using 10% concentrated HCl as this is the legally allowed concentration in my country. I know this has a lot of water but it is all I have and I'm not in deep enough to want or need to generate HCl gas.

I have tried many different ways of to administer to it that I've found on the forums. These range from adding the HCl straight to the base, making an acetone or ethanol /hcl solution at differing ratios, dissolving the base in acetone before adding the HCl solutions. No matter which way, I never get flakes precipitating. The only way I recover anything is to let the whole solution evaporate and it leaves a glassy looking substances that once fully dried grinds into a powder.

Why isn't it precipitating from the HCl? Is there anything I can do differently? I don't mind having to let it all evaporate, but surely this way crystalizes the impurities I want to avoid. And also, does the evaporation method have an adverse effect on the coke.

Sorry for the long post. Complete novice with this stuff. Appreciate anyone that read it all and can help.
 
Hi, this is something I’m really interested in, and I’ve read all kinds of threads here. But honestly, I’m not sure it actually helped me much. I’d also like to clean my stuff and get it back into a powder form. It seems complicated, but maybe it isn’t. It would be great to have something like a simple guide — clear and straightforward. I know I didn’t really give any advice here, sorry… but I’d like to follow the discussion. Maybe someone more experienced will share their thoughts
 
After some bad experiences with side effects like an extremely sore nose and bad comedowns I ended up on a le junk and David le rabbit hole to try and get rid of some the sh*t in my gear.

I've done an acetone wash and a/b procedure (somewhat successfully I believe) which leaves me with freebase. Turning it back into a snortable sort is where I'm getting grief.

I'm using 10% concentrated HCl as this is the legally allowed concentration in my country. I know this has a lot of water but it is all I have and I'm not in deep enough to want or need to generate HCl gas.

I have tried many different ways of to administer to it that I've found on the forums. These range from adding the HCl straight to the base, making an acetone or ethanol /hcl solution at differing ratios, dissolving the base in acetone before adding the HCl solutions. No matter which way, I never get flakes precipitating. The only way I recover anything is to let the whole solution evaporate and it leaves a glassy looking substances that once fully dried grinds into a powder.

Why isn't it precipitating from the HCl? Is there anything I can do differently? I don't mind having to let it all evaporate, but surely this way crystalizes the impurities I want to avoid. And also, does the evaporation method have an adverse effect on the coke.

Sorry for the long post. Complete novice with this stuff. Appreciate anyone that read it all and can help.
Typically salting out is done with gaseous HCl while your (depreciated) compound is in the non-polar fraction.

HCl gas can be created by dripping sulfuric acid onto table salt in a sealed vessel with tubing allowing you to dispense the gas into the non-polar fraction. Drip small amounts so that you don’t poison yourself, as acid gasses are hell on the throat and lungs.

Because there are no transformations of the cocaine molecule this is acceptable to discuss here .
 
After some bad experiences with side effects like an extremely sore nose and bad comedowns I ended up on a le junk and David le rabbit hole to try and get rid of some the sh*t in my gear.

I've done an acetone wash and a/b procedure (somewhat successfully I believe) which leaves me with freebase. Turning it back into a snortable sort is where I'm getting grief.

I'm using 10% concentrated HCl as this is the legally allowed concentration in my country. I know this has a lot of water but it is all I have and I'm not in deep enough to want or need to generate HCl gas.

I have tried many different ways of to administer to it that I've found on the forums. These range from adding the HCl straight to the base, making an acetone or ethanol /hcl solution at differing ratios, dissolving the base in acetone before adding the HCl solutions. No matter which way, I never get flakes precipitating. The only way I recover anything is to let the whole solution evaporate and it leaves a glassy looking substances that once fully dried grinds into a powder.

Why isn't it precipitating from the HCl? Is there anything I can do differently? I don't mind having to let it all evaporate, but surely this way crystalizes the impurities I want to avoid. And also, does the evaporation method have an adverse effect on the coke.

Sorry for the long post. Complete novice with this stuff. Appreciate anyone that read it all and can help.
After some bad experiences with side effects like an extremely sore nose and bad comedowns I ended up on a le junk and David le rabbit hole to try and get rid of some the sh*t in my gear.

I've done an acetone wash and a/b procedure (somewhat successfully I believe) which leaves me with freebase. Turning it back into a snortable sort is where I'm getting grief.

I'm using 10% concentrated HCl as this is the legally allowed concentration in my country. I know this has a lot of water but it is all I have and I'm not in deep enough to want or need to generate HCl gas.

I have tried many different ways of to administer to it that I've found on the forums. These range from adding the HCl straight to the base, making an acetone or ethanol /hcl solution at differing ratios, dissolving the base in acetone before adding the HCl solutions. No matter which way, I never get flakes precipitating. The only way I recover anything is to let the whole solution evaporate and it leaves a glassy looking substances that once fully dried grinds into a powder.

Why isn't it precipitating from the HCl? Is there anything I can do differently? I don't mind having to let it all evaporate, but surely this way crystalizes the impurities I want to avoid. And also, does the evaporation method have an adverse effect on the coke.

Sorry for the long post. Complete noviceDr.
COCAINE PURIFICATION: ONLY IF THIS IS ACCEPTABLE TO TALK ABOUT HERE? I’M GONNA TALK ABOUT IT ANYWAY……HA… Get a metal dining spoon. Average size, not too big or small. Bend the spoon end slightly so that when you sit the spoon on a table, the spoon side is perfectly horizontal. This will make sure it doesn't spill when you have to sit the spoon down.
Poor Ammonia into the spoon, about 2/3rds full. Make sure it is Ammonia from a hardware store which is already diluted with water. Also make sure the only ingredients in the bottle are pure Ammonia and water. This stuff is incredibly strong, even the diluted stuff. So make sure you don't breathe in the fumes and don't spill it anywhere. If you do then clean it up immediately.
Immerse approx 1 gram Cocaine into the Ammonia by pooring it from the bag directly into the spoon.
Immediately start to heat the solution from beneath the spoon using a standard lighter. Drift the flame in a circular motion around the base of the spoon whilst very steadily gliding the spoon itself back, forth, left and right. This will help the solution collect in the center of the spoon.
What you should see happening is the fucking powder Cocaine gathering together and slowly forming a rock-type matter in the center, it will normally form a circular shape. But it isn't an issue if it's not circular.
Your lighter is likely to get very hot, so make sure you have one or two lighters to swap with so that your lighter doesn't pop.
By the time the solution starts to really bubble and spit, the Cocaine should now have fully crystallised into Freebase, and should be sat in the center of your spoon. If it hasn't formed a rock yet, put the spoon down for a minute and then heat again. You can test if it is a rock by prodding it with a pin, if it's a rock then the pin won't go into the rock and will be stuck to the spoon slightly.
Depending on what treatment has been done to the Cocaine before import will determine if it immediately turns to rock or if you get a slightly damp sludge-type solution. If it is still damp and sludgey, then you need to leave it on the side for half hour or so until it solidifies.
Poor the Ammonia away and remove the crystallized freebase, putting it on a paper towel. (Do this with gloves so that you don't get Ammonia on your hands! It will make you very ill!)
Use a kitchen towel to soak up and dry the Ammonia which is on the freebase.
Clean your spoon.
Fill your spoon with water, 2/3rds full.
Immerse the freebase in the water of the spoon and light the spoon from beneath. Slowly but surely, you will see a stream of smoke emit from the water. This is the Ammonia which is soaked into the freebase being released. Do this for a while, when it starts to bubble, stop. Then do it again. And again. You are making sure there is no Ammonia on your freebase. (Trust me, you do NOT want to smoke it with any Ammonia on.)
Remove the freebase, dry it again with a fresh bit of paper towel, poor away the water, clean the spoon and repeat step 13.
Remove the freebase again and dry it with another fresh piece of paper towel.
If you have spilt Ammonia anywhere or got it on your hands or anything then for God's sake clean it up. I'm only reiterating this point because I've learnt the hard way. It's not the sort of chemical you want to fuck around with.
Leave your freebase to dry for 24 hours if you have the patience, this will mean you'll get more bang for your buck. Some people will pop it in the microwave but I don't advise it. Others will just stick it straight in a pipe.
That is the most thorough breakdown I can give you for making Crack-Cocaine. You may have to do some trial and error at first until you understand the process and realise whats actually going on and what you're doing along the way. There are other methods but this is the quickest, most effective way.
 
After some bad experiences with side effects like an extremely sore nose and bad comedowns I ended up on a le junk and David le rabbit hole to try and get rid of some the sh*t in my gear.

I've done an acetone wash and a/b procedure (somewhat successfully I believe) which leaves me with freebase. Turning it back into a snortable sort is where I'm getting grief.

I'm using 10% concentrated HCl as this is the legally allowed concentration in my country. I know this has a lot of water but it is all I have and I'm not in deep enough to want or need to generate HCl gas.

I have tried many different ways of to administer to it that I've found on the forums. These range from adding the HCl straight to the base, making an acetone or ethanol /hcl solution at differing ratios, dissolving the base in acetone before adding the HCl solutions. No matter which way, I never get flakes precipitating. The only way I recover anything is to let the whole solution evaporate and it leaves a glassy looking substances that once fully dried grinds into a powder.

Why isn't it precipitating from the HCl? Is there anything I can do differently? I don't mind having to let it all evaporate, but surely this way crystalizes the impurities I want to avoid. And also, does the evaporation method have an adverse effect on the coke.

Sorry for the long post. Complete novice with this stuff. Appreciate anyone that read it all and can help.
YOU CAN make ethereal HCl by mixing conc. HCl into diethyl ether and drying with MgSO4 Then you just dissolve it in organic add excess of the ethereal HCl, stirr for a while and evaporate to dryness. If you do in all in ether, there is a chance your hydrochloride will precipitate.

You can also just gheto style it by dissolving your stuff in MeOH, add excess of aq. HCl and evaporate to dryness followed by washing with ether. This works on small scales because HCl has such a low molecular weight that you need only tiny volumes.
Check your compound in the end by melting point or TLC, the salt should have vastly different RF compared to the free base

I hope I explain that OK
DH TRISMEGISTUS
 
After some bad experiences with side effects like an extremely sore nose and bad comedowns I ended up on a le junk and David le rabbit hole to try and get rid of some the sh*t in my gear.

I've done an acetone wash and a/b procedure (somewhat successfully I believe) which leaves me with freebase. Turning it back into a snortable sort is where I'm getting grief.

I'm using 10% concentrated HCl as this is the legally allowed concentration in my country. I know this has a lot of water but it is all I have and I'm not in deep enough to want or need to generate HCl gas.

I have tried many different ways of to administer to it that I've found on the forums. These range from adding the HCl straight to the base, making an acetone or ethanol /hcl solution at differing ratios, dissolving the base in acetone before adding the HCl solutions. No matter which way, I never get flakes precipitating. The only way I recover anything is to let the whole solution evaporate and it leaves a glassy looking substances that once fully dried grinds into a powder.

Why isn't it precipitating from the HCl? Is there anything I can do differently? I don't mind having to let it all evaporate, but surely this way crystalizes the impurities I want to avoid. And also, does the evaporation method have an adverse effect on the coke.

Sorry for the long post. Complete novice with this stuff. Appreciate anyone that read it all and can help.
What about sulphuric acid? Conc. sulphuric (hardware) gets you quickly to relatively dry HCl, especially if you bubble first through concentrated sulphuric. Could also bubble into a non polar hydrophobic solvent that would dissolve it (hardware). Check mole calculations, lower temp to increase solubility.

Amine salts are notoriously hydrophilic, this one in particular. Amine salts often oil out due to impurity or poor crystallization methods. A simple air dry won’t do. Might be able to salvage with miscible non-polar solvents. Would depend on the water azeotrope and purity of the sample. Choose wisely and you can strip the water. Be safe.
 
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Hi, this is something I’m really interested in, and I’ve read all kinds of threads here. But honestly, I’m not sure it actually helped me much. I’d also like to clean my stuff and get it back into a powder form. It seems complicated, but maybe it isn’t. It would be great to have something like a simple guide — clear and straightforward. I know I didn’t really give any advice here, sorry… but I’d like to follow the discussion. Maybe someone more experienced will share their thoughts
It’s the last fight against water. If you’re introducing water (by adding a low concentration acid) you have to struggle against how much this thing just would prefer to stick to water than to do anything else.

If you get impatient and add heat, even worse. Hydrolysis.

If you introduce dry gas, you have to deal with its corrosion. Even if you’re careful, if not protected from water, back to that oil. So it was a fun thought but you forgot the basics.

It’s certainly not easy, the best approaches need a solid understanding of how to safely dissolve HCL into solution without eating away at your skin or target chemical. It would be quite dangerous to write this part of the recipe out, since to safely use it you’d need to understand all the why’s.

The other approaches need a better understanding of your mix, and again wouldn’t be written out.

This “tech” fails because the writer doesn't understand why it could fail so doesn’t account for systems to prevent it.
 
Hi, this is something I’m really interested in, and I’ve read all kinds of threads here. But honestly, I’m not sure it actually helped me much. I’d also like to clean my stuff and get it back into a powder form. It seems complicated, but maybe it isn’t. It would be great to have something like a simple guide — clear and straightforward. I know I didn’t really give any advice here, sorry… but I’d like to follow the discussion. Maybe someone more experienced will share their thoughts
It’s just complicated, and dangerous. Especially if you’re not sure if it’s complicated or dangerous.

Unless… you have a good setup and understand why it’s set up like that. Then you could ask why was this suggested when the larger chemistry community goes the other route for similar compounds? Was the author being lazy or just not informed? What could be changed? If you made that change, is there more or less control? Byproducts? Can you introduce a vacuum, one way valve, what step? Blowback? Runaway? How to estimate what things look like near completion? Is water getting back in?
 
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YOU CAN make ethereal HCl by mixing conc. HCl into diethyl ether and drying with MgSO4 Then you just dissolve it in organic add excess of the ethereal HCl, stirr for a while and evaporate to dryness. If you do in all in ether, there is a chance your hydrochloride will precipitate.

You can also just gheto style it by dissolving your stuff in MeOH, add excess of aq. HCl and evaporate to dryness followed by washing with ether. This works on small scales because HCl has such a low molecular weight that you need only tiny volumes.
Check your compound in the end by melting point or TLC, the salt should have vastly different RF compared to the free base

I hope I explain that OK
DH TRISMEGISTUS
 
Hehe brother he has a low conc hcl. Would the reaction even kick off unless he’s blowtorching right now?
 
Check it I can send you much better instructions with images to help guide you.... my email iz [[email protected]]
makin snow snow snow a friggin white out blizzard! BRRRR/..... email me and ill send you a perfect step by step with images 1. 2. 3. 4. etc..... jusss let me know its you from blue Ill be of great assistance.
 
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