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The Big & Dandy N,N-DMT Extraction Thread - Elves are watching

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decided to go with this but dont know where to get fumaric acid....




Materials

-Gallon Milk Jug(HDPE #2 plastic)
-Two 800ml(as close as you can) glass jar
-One 100ml(also as close as you can get) glass jar
-250g Sodium Hydroxide
-About 5g of Fumaric Acid(probably way more than enough but whatever)
-1 liter of 5% vinegar
-450g(one pound) of powdered Mimosa hostilis root bark
-473ml(16fl oz) bottle of 99% IPA
-ABOUT 2.5 liters of water
-500ml of D-limonene(100ml per pull)

The Process

Step One: Take your gallon jug and pour 1 liter of vinegar into it. Then add your pound of bark. Shake this hard to get it all mixed up. Then put it somewhere and let it sit for 3 days.

Step Two: WEAR GLASSES. Add 500ml water to one of the large glass jars. Then slowly and carefully add 250g sodium hydroxide to it. Make sure this all gets absorbed into the water. Then after the lye water solution has cooled down, pour this into your gallon milk jug that has the vinegar and root bark in it. Then add around 1.75 liters of water to the jug to top it off(you want enough room at the top for 100ml of d-limonene). Now mix this together very well.

Step Three: Add 100ml of d-limonene to the gallon jug and mix it together. Don't shake it, just mix it end over end gently. Be careful to keep the cap on the milk jug. The first 2 pulls can be done in about 1-2 hours. After about an hour of mixing then separating and mixing and separating, pull as much of the d-limonene off the top as you can and put it into the other big glass jar. Do this again with another 100ml of d-limonene, mixing for an hour then pulling. The next three 100ml pulls will need to sit for a while longer to make sure you get all the dmt. Do at least one pull a day for three days. Mixing as often as you think about it. Add each pull to the dmt d-limonene jar.

Step Four: Take your small jar and put 5g fumaric acid in it and then fill the jar with your 99% IPA. Then mix this together until the IPA is completely saturated. This creates Fumaric Acid Saturated IPA(FASI). Most likely you will have excess fumaric acid on the bottom but that is fine. Now SLOWLY pour your FASI into your jar of dmt saturated d-limonene. The slower the better. For best results add 10ml FASI every 5 minutes until you dont see any more cloud forming in the d-limonene. This will crash out your dmt from the d-limonene. Allow this to sit for at least 24 hours after you stop putting in FASI so that the DMT Fumarate can fully crash out. After 24 hours add another 1ml of FASI to make sure all dmt has precipitated out. After you collect the DMT fumarate from the jar, put the d-limonene back into the jar and let it sit for a few days. More DMT fumarate will precipitate over time.

Step Five: Pour off the d-limonene from your now beautiful crystals. Turn the jar upside down and put it on a paper towel to absorb any extra D-Limonene that falls out. Allow this to sit out until it dries a bit more. You can use a bit of heat and a fan to speed this process up. Now scrape up your JIMJAM fumarate. It will smell mildly of oranges. DONE
 
Pickle, it should be noted that the first two teks you listed are essentially the same. They're both STB. The only major difference is the freeze precipitation step, which I consider essential. Simply evaporating the naptha will yield a much dirtier product.

Also, the last one you listed will yield dmt fumarate, which isn't really usable by vaporization.
 
Shakti said:
Pickle, it should be noted that the first two teks you listed are essentially the same. They're both STB. The only major difference is the freeze precipitation step, which I consider essential. Simply evaporating the naptha will yield a much dirtier product.

Also, the last one you listed will yield dmt fumarate, which isn't really usable by vaporization.
Click to expand...

i can't smoke it you mean?????
 
I did another extraction on that North Brazilian MHRB and I got a 1,58% yield after freeze precipitation.

On the other hand, I'm having trouble producing pure white spice. It is snow white when I pour off the naphtha after recrystallization, but by the time it dries (I leave it to air dry for 12-24 hrs.) it is already off-white.
 
RigaCrypto said:
I did another extraction on that North Brazilian MHRB and I got a 1,58% yield after freeze precipitation.

On the other hand, I'm having trouble producing pure white spice. It is snow white when I pour off the naphtha after recrystallization, but by the time it dries (I leave it to air dry for 12-24 hrs.) it is already off-white.
Click to expand...

that one seems harder
 
^ Why not? As long as you have access to a pipe, you can smoke it (on herbs, ash, or chore boy).
 
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