cletusSamboy
Bluelighter
- Joined
- Oct 24, 2021
- Messages
- 420
I've tried an acid base extraction technique I found here but I can't get the acid/solvent mixture to freeze for seperation (step 9).
Is this method correct or have I just wasted my meth?
1. Add 20ml water in jar.
2. Add sodium hydroxide solution (mixed in water) to meth/water mix. Add sodium hydroxide to water not water to sodium hydroxide. Do it slowly. Stir.
3. Add 10ml shellite to the solution.
4. Stir solution.
5. Freeze solution. Water will freeze and other liquids can be seperated from water.
6. Pour unfrozen shellite into seperate jar.
7. Keep the sodium/meth water/ice in first glass.
8. Add 10ml 37% hydrochloric acid into jar with shellite.
9. Shake it then freeze to seperate.
10. Pour back into first glass. Use ice cold water to rinse solvent from the ice. Pour into first glass.
11. Let ice in second glass melt and evaporate. Powder is pure meth.
12. Repeat above steps until no more meth appears.
So it won't freeze but I've managed to draw off the solvent from the top of the acid and have left the acid to sit to slow evaporate. It's been nearly a month and nothing is evaporating. My meth should be in the acid but how can I get this out if it won't evaporate?
Is this method correct or have I just wasted my meth?
1. Add 20ml water in jar.
2. Add sodium hydroxide solution (mixed in water) to meth/water mix. Add sodium hydroxide to water not water to sodium hydroxide. Do it slowly. Stir.
3. Add 10ml shellite to the solution.
4. Stir solution.
5. Freeze solution. Water will freeze and other liquids can be seperated from water.
6. Pour unfrozen shellite into seperate jar.
7. Keep the sodium/meth water/ice in first glass.
8. Add 10ml 37% hydrochloric acid into jar with shellite.
9. Shake it then freeze to seperate.
10. Pour back into first glass. Use ice cold water to rinse solvent from the ice. Pour into first glass.
11. Let ice in second glass melt and evaporate. Powder is pure meth.
12. Repeat above steps until no more meth appears.
So it won't freeze but I've managed to draw off the solvent from the top of the acid and have left the acid to sit to slow evaporate. It's been nearly a month and nothing is evaporating. My meth should be in the acid but how can I get this out if it won't evaporate?
Last edited: