Hello every dear bluelighters !
I'm currently in the process of a harmaline/harmine extraction from 200g syrian rue. That's such a fucking nightmare to filtering the sludge from goodies. That's why I was thinking of an extraction using naphta or toluene like the DMT extraction.
1. Extracting the harmala salts using an acidic solution (water + vinegar).
2. NO FILTERING
3. Basifing the aqueous solution using NaOH or sodium carbonate.
4. Pull the freebase alkaloids from the basified aqueous solution with naphta or xylene.
5. Shake well an separate the two layers.
6. Freezing the naphta or xylene to precipitate harmalas ; or if it don't work like DMT, evaporate the naphta.
In this way, all the vegetal materials will be left on the basified aqueous solution (3).
Did somebody succeed to do that already?
Thanks a lot for your answers ! Peace and happy drugging for all
I'm currently in the process of a harmaline/harmine extraction from 200g syrian rue. That's such a fucking nightmare to filtering the sludge from goodies. That's why I was thinking of an extraction using naphta or toluene like the DMT extraction.
1. Extracting the harmala salts using an acidic solution (water + vinegar).
2. NO FILTERING
3. Basifing the aqueous solution using NaOH or sodium carbonate.
4. Pull the freebase alkaloids from the basified aqueous solution with naphta or xylene.
5. Shake well an separate the two layers.
6. Freezing the naphta or xylene to precipitate harmalas ; or if it don't work like DMT, evaporate the naphta.
In this way, all the vegetal materials will be left on the basified aqueous solution (3).
Did somebody succeed to do that already?
Thanks a lot for your answers ! Peace and happy drugging for all