GeekinB3AST
Bluelighter
- Joined
- Mar 12, 2017
- Messages
- 66
Can somone prefferably a Mod or a Veteran member please verify that this is correct and im not going to fucking kill myself, much appreciated
NOTE:GIB =METH
GIB Purification through Re-crystallization
Materials:
- 3 glass containers
- Pot/Pan large enough to 3 fit glass containers
- Bowl to contain ice water for cooling of single glass container
- Denatured Alcohol (Home Depot: Klean Strip Denatured Alcohol)
- Acetone (Home Depot: Klean-Strip Aceton)
- Filter: Coffee filter unbleached (preferable)
Prep:
- Freeze Acetone
- Clean containers
- Crush GIB into powder
- Bring water to simmer 70? C/158*F in pot/pan
Procedure:
1) Heat Denatured Alcohol
- Place ? - ? cup Alcohol in a glass container and heat in simmer water. Keep hot but regulate to prevent excessive boiling (flammable fumes).
-Note: Denatured Alcohol boils at 56? C./132.8*F
2) Place crush GIB in another glass container and place in the water.
3) Add 2ml denatured alcohol per 1gram GIB
- 2ml/gram - Alcohol:GIB ratio
a) Technique:
- Remove container from water for dissolving.
- Reheat container and/or introduce additional alcohol (? ml/gram) if further dissolving is needed.
4) Continue simmer Alcohol-GIB solution on low heat.
5) Action Item : Re-Dissolve
- Trigger: Skin/Crystals starts forming upon evaporation of Alcohol
- Response: Add ? - 1ml/gram until completely dissolved
6) Action Item (Repeat ~3 times) : Addition of Acetone
- Trigger: Skin/Crystals starts forming upon evaporation of Alcohol
- Response: Add 1ml increments of *freezer cold* acetone. Make sure crystals are at least covered.
a) Technique:
- Swirl to agitate crystal
- Keep acetone container sealed as long as possible, acetone absorbs moisture from the air.
- Do not evaporate last addition of acetone see step 7
b) Why:
- The point is to evaporate off the alcohol, while slowly bringing back the crystals in the acetone
7) With last acetone addition in step 6, do not evaporate fully. Crystals should be able to freely move in liquid.
8) Place Acetone-gib container in a bowl of Iced water to prevent further evaporation
9) Add 5-6 ml(0.34TBSP-0.41TBSP) Acetone to container
10) Filter gib through filter into 3rd glass container.
- Wash any remaining particles out of container with acetone into filter
- Contents trapped in filter is Gib
- Liquid filtered through is acetone (discard with running water)
11) Air dry gib (15-20 minutes)
12) Repeat Step 9 -> 11 for additional purification.
METHOD 2
Drying Acetone
⦁ Acetone
⦁ Epsom salts
⦁ Filter paper (coffee filters work fine)
⦁ Oven
⦁
Most acetone that youll buy will be dry enough to use for washing. Though the older it is the greater the chance it has absorbed moisture from the air.
Put some of the Epsom salts on a tray in the oven for an hour or so on at least 130 degrees Centigrade.(266 F ) (This is to dry any moisture out of them)
Pour the Epsom salts into the acetone and mix them around.
Filter the acetone through the filter paper.
Ideally, use the acetone soon, to avoid it re-absorbing more moisture.
Acetone Wash
Youll Need:
⦁ Acetone (really cold, to avoid losses)*Like do i put the Anhydrous Acetone in the freezer?
⦁ Bowl (ideally glass, shallow & with straight sides. Not too wide either, 4inch[10cm] is a good size)
⦁ Knife
Instructions:
[*]Put the Meth in bowl.
[*]Add the cold acetone 30-50mL is usually enough for ?-1gram
[*]Swish the bowl around and then use the knife to break up any larger bits of impurities A minute or so will be fine.
[*]Tip the bowl onto an angle and swish it around so that all of the meth is together in a corner.
[*]Let it settle out for a short while, then SLOWLY tip the bowl around so that the meth stays in the corner and the acetone drains off and is now on the other side of the bowl.
[*]The acetone can be poured off or you can leave the bowl propped up on an angle and let it evaporate. A small amount of meth will be in the acetone. You can pour it off into another bowl and then do more acetone washes on it if you want.
More acetone washes can be performed if it still looks to be dirty. Ideally, you should recrystalise the meth in between acetone washes (and even before the first wash)[/list]
Clean meth is a white-ish/cloudy crystal that will give off white vapour when heated
Recrystalisation
⦁ Bowl (same as the one above)
⦁ Ethanol (Methylated Spirits works fine) *HEET?
⦁ Knife
[*]Put the meth in the bowl
[*]Heat a small amount of Methylated Spirits( I have HEET will this work?) (a glass in the microwave works, just dont put it on for too long]
[*]Meth is quite soluble in Methylated Spirits, so you want to use as little as possible. 20-30mL for ½ gram
[*]Swish it around and then use the knife to help break up any bits that wont dissolve.
[*]Some of the impurities will dissolve, some wont. If youre unsure, add a tiny bit more Methylated Spirits and see if any more dissolves. If not then its probably an impurity.
If there are undissolved impurities, tip the bowl onto an angle and swish it around so that all the impurities are together in a corner.
[*]Let it settle out for a while, then SLOWLY tip the bowl around so that the crap stays where it is and the Methylated Spirits drains off it and is now on the other side of the bowl.
*]Scrape the crap out of the bowl.
NOTE:GIB =METH
GIB Purification through Re-crystallization
Materials:
- 3 glass containers
- Pot/Pan large enough to 3 fit glass containers
- Bowl to contain ice water for cooling of single glass container
- Denatured Alcohol (Home Depot: Klean Strip Denatured Alcohol)
- Acetone (Home Depot: Klean-Strip Aceton)
- Filter: Coffee filter unbleached (preferable)
Prep:
- Freeze Acetone
- Clean containers
- Crush GIB into powder
- Bring water to simmer 70? C/158*F in pot/pan
Procedure:
1) Heat Denatured Alcohol
- Place ? - ? cup Alcohol in a glass container and heat in simmer water. Keep hot but regulate to prevent excessive boiling (flammable fumes).
-Note: Denatured Alcohol boils at 56? C./132.8*F
2) Place crush GIB in another glass container and place in the water.
3) Add 2ml denatured alcohol per 1gram GIB
- 2ml/gram - Alcohol:GIB ratio
a) Technique:
- Remove container from water for dissolving.
- Reheat container and/or introduce additional alcohol (? ml/gram) if further dissolving is needed.
4) Continue simmer Alcohol-GIB solution on low heat.
5) Action Item : Re-Dissolve
- Trigger: Skin/Crystals starts forming upon evaporation of Alcohol
- Response: Add ? - 1ml/gram until completely dissolved
6) Action Item (Repeat ~3 times) : Addition of Acetone
- Trigger: Skin/Crystals starts forming upon evaporation of Alcohol
- Response: Add 1ml increments of *freezer cold* acetone. Make sure crystals are at least covered.
a) Technique:
- Swirl to agitate crystal
- Keep acetone container sealed as long as possible, acetone absorbs moisture from the air.
- Do not evaporate last addition of acetone see step 7
b) Why:
- The point is to evaporate off the alcohol, while slowly bringing back the crystals in the acetone
7) With last acetone addition in step 6, do not evaporate fully. Crystals should be able to freely move in liquid.
8) Place Acetone-gib container in a bowl of Iced water to prevent further evaporation
9) Add 5-6 ml(0.34TBSP-0.41TBSP) Acetone to container
10) Filter gib through filter into 3rd glass container.
- Wash any remaining particles out of container with acetone into filter
- Contents trapped in filter is Gib
- Liquid filtered through is acetone (discard with running water)
11) Air dry gib (15-20 minutes)
12) Repeat Step 9 -> 11 for additional purification.
METHOD 2
Drying Acetone
⦁ Acetone
⦁ Epsom salts
⦁ Filter paper (coffee filters work fine)
⦁ Oven
⦁
Most acetone that youll buy will be dry enough to use for washing. Though the older it is the greater the chance it has absorbed moisture from the air.
Put some of the Epsom salts on a tray in the oven for an hour or so on at least 130 degrees Centigrade.(266 F ) (This is to dry any moisture out of them)
Pour the Epsom salts into the acetone and mix them around.
Filter the acetone through the filter paper.
Ideally, use the acetone soon, to avoid it re-absorbing more moisture.
Acetone Wash
Youll Need:
⦁ Acetone (really cold, to avoid losses)*Like do i put the Anhydrous Acetone in the freezer?
⦁ Bowl (ideally glass, shallow & with straight sides. Not too wide either, 4inch[10cm] is a good size)
⦁ Knife
Instructions:
[*]Put the Meth in bowl.
[*]Add the cold acetone 30-50mL is usually enough for ?-1gram
[*]Swish the bowl around and then use the knife to break up any larger bits of impurities A minute or so will be fine.
[*]Tip the bowl onto an angle and swish it around so that all of the meth is together in a corner.
[*]Let it settle out for a short while, then SLOWLY tip the bowl around so that the meth stays in the corner and the acetone drains off and is now on the other side of the bowl.
[*]The acetone can be poured off or you can leave the bowl propped up on an angle and let it evaporate. A small amount of meth will be in the acetone. You can pour it off into another bowl and then do more acetone washes on it if you want.
More acetone washes can be performed if it still looks to be dirty. Ideally, you should recrystalise the meth in between acetone washes (and even before the first wash)[/list]
Clean meth is a white-ish/cloudy crystal that will give off white vapour when heated
Recrystalisation
⦁ Bowl (same as the one above)
⦁ Ethanol (Methylated Spirits works fine) *HEET?
⦁ Knife
[*]Put the meth in the bowl
[*]Heat a small amount of Methylated Spirits( I have HEET will this work?) (a glass in the microwave works, just dont put it on for too long]
[*]Meth is quite soluble in Methylated Spirits, so you want to use as little as possible. 20-30mL for ½ gram
[*]Swish it around and then use the knife to help break up any bits that wont dissolve.
[*]Some of the impurities will dissolve, some wont. If youre unsure, add a tiny bit more Methylated Spirits and see if any more dissolves. If not then its probably an impurity.
If there are undissolved impurities, tip the bowl onto an angle and swish it around so that all the impurities are together in a corner.
[*]Let it settle out for a while, then SLOWLY tip the bowl around so that the crap stays where it is and the Methylated Spirits drains off it and is now on the other side of the bowl.
*]Scrape the crap out of the bowl.