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2CB Fail

The page indeed provides a method to purity the HBr. It is not a big deal to do so if you have a proper laboratory, you might as well just do a column chromatography. If you have a proper lab, Shulgin's choice is obvious. The only reason I can see for cleaning the HBr salt is that you not able to distill the free base. With a vacuum pump this is absolutely safe and I can not support the reasoning from the page against it.

It would be interesting if one of our beloved Dutch members could run a lab test on tanned HBr salt to establish the purity.

Waffle-head: very impressive. Did you give a sample of every blotter to a lab?
 
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