Ineffable14
Bluelighter
- Joined
- May 15, 2012
- Messages
- 238
I was going through the archives and various sources and found this--
"Dpt hydrochloride in ethanol or isopropanol (may require a bit of heat). Also dissolve NaOH in isopropanol or ethanol (1g in 200ml then store in airtight plastic container). For every 30mg of DPT hydrochloride you need 5mg of NaOH to fully convert it to freebase. For say 300mg of DPT in solution in 30ml of isopropanol or ethanol you'll require 10ml of the above alcoholic NaOH solution (1g in 200ml = 5mg/ml. 300mg DPT.HCl requires 50mg NaOH which works out at 10ml of solution). You simply mix them together, warm the solution and leave it for an hour. In the space of that hour the DPT.HCl + NaOH converts to DPT (freebase) and NaCl (plus a tiny - insignificant - amount of water). NaCl is common salt and is utterly insoluble in alcohol, so it makes the liquid appear cloudy. You don't even need to remove the NaCl to smoke it as it's inert at the temp used to vapourize DPT freebase."
It was my understanding that the freebase would have to be pulled from the solution as it would result in the final product containing some amounts of NaOH. Does this process fully convert the lye to the inert NaCl? Would this same process work using 99% iso ethanol considering there is some water content?
Also how long will the resulting oil hold potency in a freezer?
Thanks ahead for any input!
Cheers
"Dpt hydrochloride in ethanol or isopropanol (may require a bit of heat). Also dissolve NaOH in isopropanol or ethanol (1g in 200ml then store in airtight plastic container). For every 30mg of DPT hydrochloride you need 5mg of NaOH to fully convert it to freebase. For say 300mg of DPT in solution in 30ml of isopropanol or ethanol you'll require 10ml of the above alcoholic NaOH solution (1g in 200ml = 5mg/ml. 300mg DPT.HCl requires 50mg NaOH which works out at 10ml of solution). You simply mix them together, warm the solution and leave it for an hour. In the space of that hour the DPT.HCl + NaOH converts to DPT (freebase) and NaCl (plus a tiny - insignificant - amount of water). NaCl is common salt and is utterly insoluble in alcohol, so it makes the liquid appear cloudy. You don't even need to remove the NaCl to smoke it as it's inert at the temp used to vapourize DPT freebase."
It was my understanding that the freebase would have to be pulled from the solution as it would result in the final product containing some amounts of NaOH. Does this process fully convert the lye to the inert NaCl? Would this same process work using 99% iso ethanol considering there is some water content?
Also how long will the resulting oil hold potency in a freezer?
Thanks ahead for any input!
Cheers