Because I am weak in English, I use the machine translation.
I took in 3,4-Ethylenedioxypyrovalerone(EDPV) and an estimated material.
This material is analog of MDPV.
IUPAC name: 1-(2,3-dihydro-1,4-benzodioxin-6-yl)-2-(pyrrolidin-1-yl)pentan-1-one hydrochloride
Purity: Unconfirmed
A color: Considerably white
A factory: My home
I'm a man of weight 78kg (172 lb).
I dissolved 10 mg of EDPV hydrochloride per water 1mL.
T+00:00
I mixed 3 mg in Red Bull and drank.
Several minutes later, I had a buzzing in my ears.
Some feelings became bright when it passed more than ten minutes.
Pupillary size does not have the change.
T+00:30
I mixed 5 mg in Red Bull and drank.
T+01:30
I mixed 10 mg to cafe au lait and drank.
Pupillary size does not have the change.
I came to want food of the saltiness. I ate a dry sausage.
T+03:00
There is no pupillary change.
T+03:30 - 04:10
I mixed 10 mg to cafe au lait and drank for 40 minutes.
T+05:00
Mild bruxism.
Bowel movement (not diarrhea).
T+06:20
It is taken in 5 mg by rectum.
(5 mg enters the water of 3mL)
T+07:00
I mixed 12 mg in isotonic drink and drank.
I took in 45 mg in total.
However, there was not feeling of awakening.
Probably this is not "a stimulant".
After having taken the sleep enough, I urinated.
The urine smells of ammonia.
When I put hydrochloride in a glass pipe and heat up, some brown materials stay.
However, probably the vaporization is possible.
When I inhaled several mg, there was only light ringing in the ears.
The pupil did not open.
Synthesis
1, Friedel Crafts acylation
I mixed 1,4-Benzodioxane and Valeryl Chloride and Zinc Oxide.
2, Vacuum distillation
At low temperature, a material thought to be 2,3-Ethylenedioxyvalerophenone was provided in small quantities.
It is a liquid at room temperature.
At high temperature, a material thought to be 3,4-Ethylenedioxyvalerophenone was provided in large quantities.
It is a liquid at first, but gradually crystallizes.
3, Bromination
I mixed p-Toluenesulfonic Acid Monohydrate and N-Bromosuccinimide with 3,4-Ethylenedioxyvalerophenone and heated up.
4, Amination
I mixed Pyrrolidine with 3,4-Ethylenedioxybromovalerophenone.
A yield: 8.16 g (HCl)
Yield: 25% (with Benzodioxane a standard)
This photo shows 3,4-Ethylenedioxyvalerophenone.
Tagged by Xorkoth
substancecode_edpv
substancecode_pyrovalerones
substancecode_stimulants
explevel_firsttime
exptype_neutral
roacode_oral
roacode_vaporized
roacode_inhaled
I took in 3,4-Ethylenedioxypyrovalerone(EDPV) and an estimated material.
This material is analog of MDPV.
IUPAC name: 1-(2,3-dihydro-1,4-benzodioxin-6-yl)-2-(pyrrolidin-1-yl)pentan-1-one hydrochloride
Purity: Unconfirmed
A color: Considerably white
A factory: My home
I'm a man of weight 78kg (172 lb).
I dissolved 10 mg of EDPV hydrochloride per water 1mL.
T+00:00
I mixed 3 mg in Red Bull and drank.
Several minutes later, I had a buzzing in my ears.
Some feelings became bright when it passed more than ten minutes.
Pupillary size does not have the change.
T+00:30
I mixed 5 mg in Red Bull and drank.
T+01:30
I mixed 10 mg to cafe au lait and drank.
Pupillary size does not have the change.
I came to want food of the saltiness. I ate a dry sausage.
T+03:00
There is no pupillary change.
T+03:30 - 04:10
I mixed 10 mg to cafe au lait and drank for 40 minutes.
T+05:00
Mild bruxism.
Bowel movement (not diarrhea).
T+06:20
It is taken in 5 mg by rectum.
(5 mg enters the water of 3mL)
T+07:00
I mixed 12 mg in isotonic drink and drank.
I took in 45 mg in total.
However, there was not feeling of awakening.
Probably this is not "a stimulant".
After having taken the sleep enough, I urinated.
The urine smells of ammonia.
When I put hydrochloride in a glass pipe and heat up, some brown materials stay.
However, probably the vaporization is possible.
When I inhaled several mg, there was only light ringing in the ears.
The pupil did not open.
Synthesis
1, Friedel Crafts acylation
I mixed 1,4-Benzodioxane and Valeryl Chloride and Zinc Oxide.
2, Vacuum distillation
At low temperature, a material thought to be 2,3-Ethylenedioxyvalerophenone was provided in small quantities.
It is a liquid at room temperature.
At high temperature, a material thought to be 3,4-Ethylenedioxyvalerophenone was provided in large quantities.
It is a liquid at first, but gradually crystallizes.
3, Bromination
I mixed p-Toluenesulfonic Acid Monohydrate and N-Bromosuccinimide with 3,4-Ethylenedioxyvalerophenone and heated up.
4, Amination
I mixed Pyrrolidine with 3,4-Ethylenedioxybromovalerophenone.
A yield: 8.16 g (HCl)
Yield: 25% (with Benzodioxane a standard)
This photo shows 3,4-Ethylenedioxyvalerophenone.
Tagged by Xorkoth
substancecode_edpv
substancecode_pyrovalerones
substancecode_stimulants
explevel_firsttime
exptype_neutral
roacode_oral
roacode_vaporized
roacode_inhaled
Last edited:
