Doclad
Bluelighter
- Joined
- Mar 17, 2015
- Messages
- 415
Greetings.
I'll be quick.
1. I bought 3-mmc. I analyzed it (GC/MS), the result was 63% purity.
2. I washed it with anhydrous acetone. I analyzed it again (GC/MS), the result was 65%.
3. I wanted to go further. I made an A/B extraction with HCl to make sure to obtain a high purity percentage. I sent it back to analyze (GC / MS), the result was 65%.
I have lost half of my product trying to purify a substance that shows the same percentage of purity after an A/B extraction.
What can be happening here?
DocLad
I'll be quick.
1. I bought 3-mmc. I analyzed it (GC/MS), the result was 63% purity.
2. I washed it with anhydrous acetone. I analyzed it again (GC/MS), the result was 65%.
3. I wanted to go further. I made an A/B extraction with HCl to make sure to obtain a high purity percentage. I sent it back to analyze (GC / MS), the result was 65%.
I have lost half of my product trying to purify a substance that shows the same percentage of purity after an A/B extraction.
What can be happening here?
DocLad